Peptide and Protein Dynamics and Low-Temperature/DNP Magic Angle Spinning NMR

In DNP MAS NMR experiments at ∼80–110 K, the structurally important −¹³CH₃ and −¹⁵NH₃⁺ signals in MAS spectra of biological samples disappear due to the interference of the molecular motions with the ¹H decoupling. Here we investigate the effect of these dynamic processes on the NMR line shapes and...

Full description

Saved in:
Bibliographic Details
Main Authors: Daviso, Eugenio, Herzfeld, Judith, Ni, Qing Zhe, Markhasin, Evgeny, Can, Thach V, Corzilius, Bjorn, Tan, Kong Ooi, Barnes, Alexander, Su, Yongchao, Griffin, Robert Guy
Other Authors: Francis Bitter National Magnet Laboratory
Format: Article
Language:en_US
Published: American Chemical Society (ACS) 2018
Online Access:http://hdl.handle.net/1721.1/115108
https://orcid.org/0000-0001-9092-612X
https://orcid.org/0000-0003-1589-832X

CIC - Centro de Información y Conocimiento Johannes Gutenberg ®