Peptide and Protein Dynamics and Low-Temperature/DNP Magic Angle Spinning NMR

In DNP MAS NMR experiments at ∼80–110 K, the structurally important −¹³CH₃ and −¹⁵NH₃⁺ signals in MAS spectra of biological samples disappear due to the interference of the molecular motions with the ¹H decoupling. Here we investigate the effect of these dynamic processes on the NMR line shapes and...

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Bibliographic Details
Main Authors: Daviso, Eugenio, Herzfeld, Judith, Ni, Qing Zhe, Markhasin, Evgeny, Can, Thach V, Corzilius, Bjorn, Tan, Kong Ooi, Barnes, Alexander, Su, Yongchao, Griffin, Robert Guy
Other Authors: Francis Bitter National Magnet Laboratory
Format: Article
Published: American Chemical Society (ACS) 2018
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